袁洪娟
發布時間: 2024-06-14 15:18
摘要:一段轉化(hua)爐煙(yan)(yan)氣(qi)中(zhong)(zhong)氮(dan)(dan)氧(yang)化(hua)物(wu)超(chao)標對環境造成極(ji)大危(wei)害,分析(xi)煙(yan)(yan)氣(qi)中(zhong)(zhong)氮(dan)(dan)氧(yang)化(hua)物(wu)的來源及氮(dan)(dan)氧(yang)化(hua)物(wu)超(chao)標的原因。通過采取(qu)相應的優化(hua)對策,控制(zhi)尾(wei)氣(qi)中(zhong)(zhong)氨含量就能有(you)效控制(zhi)煙(yan)(yan)氣(qi)中(zhong)(zhong)氮(dan)(dan)氧(yang)化(hua)物(wu)含量,從而(er)成功解決了煙(yan)(yan)氣(qi)中(zhong)(zhong)氮(dan)(dan)氧(yang)化(hua)物(wu)含量超(chao)標問題(ti)。 關鍵詞:一段轉化(hua)爐 煙(yan)(yan)氣(qi) 氮(dan)(dan)氧(yang)化(hua)物(wu) 弛(chi)放氣(qi) 尾(wei)氣(qi)
發布時間(jian): 2024-05-17 16:00
發布時間: 2024-05-09 16:32
作(zuo)(zuo)(zuo)者:張仕奇(qi)。 作(zuo)(zuo)(zuo)者簡介:張仕奇(qi),男(nan),1990年2月出生(sheng),本(ben)科學歷,工(gong)程(cheng)(cheng)師(shi),2013年畢(bi)業(ye)于遼寧石油化(hua)工(gong)大學化(hua)學工(gong)程(cheng)(cheng)與(yu)工(gong)藝專業(ye),現在(zai)阿克(ke)蘇華錦化(hua)肥有(you)(you)限責(ze)任公司(si)合成(cheng)車間從事設(she)備管(guan)(guan)理工(gong)作(zuo)(zuo)(zuo)。 摘(zhai)要:介紹合成(cheng)氨裝(zhuang)置一段(duan)(duan)(duan)轉(zhuan)化(hua)爐(lu)爐(lu)管(guan)(guan)的改(gai)造(zao)更新情況,從爐(lu)管(guan)(guan)金屬組(zu)織在(zai)不同服役(yi)時(shi)間的狀態、爐(lu)管(guan)(guan)材(cai)質、使用(yong)過(guo)程(cheng)(cheng)中可能對爐(lu)管(guan)(guan)壽(shou)命(ming)(ming)產(chan)生(sheng)影(ying)響的主要事件、不同有(you)(you)害因(yin)素對爐(lu)管(guan)(guan)使用(yong)壽(shou)命(ming)(ming)的影(ying)響等(deng)方面進行(xing)了分析(xi)探(tan)討,提出了爐(lu)管(guan)(guan)運行(xing)調(diao)整中應注意的事項。 關(guan)鍵詞:一段(duan)(duan)(duan)轉(zhuan)化(hua)爐(lu)?爐(lu)管(guan)(guan)材(cai)質?金屬組(zu)織?過(guo)熱損傷?使用(yong)壽(shou)命(ming)(ming) 1??概述(shu) 阿克(ke)蘇華錦化(hua)肥有(you)(you)限責(ze)任公司(si)一段(duan)(duan)(duan)轉(zhuan)化(hua)爐(lu)為凱(kai)洛(luo)格型合成(cheng)氨工(gong)藝轉(zhuan)化(hua)爐(lu),由(you)輻射(she)段(duan)(duan)(duan)、對流段(duan)(duan)(duan)和通(tong)(tong)風(feng)系(xi)統(tong)組(zu)成(cheng),采用(yong)強制通(tong)(tong)風(feng)方式,爐(lu)膛輻射(she)段(duan)(duan)(duan)有(you)(you)378根(gen)(gen)爐(lu)管(guan)(guan),分成(cheng)9排(pai),每(mei)(mei)排(pai)42根(gen)(gen)爐(lu)管(guan)(guan)底部與(yu)下(xia)集(ji)氣管(guan)(guan)連(lian)通(tong)(tong),在(zai)每(mei)(mei)根(gen)(gen)下(xia)集(ji)氣管(guan)(guan)中部有(you)(you)1根(gen)(gen)上升管(guan)(guan),通(tong)(tong)過(guo)下(xia)集(ji)氣管(guan)(guan)匯集(ji)工(gong)藝氣體沿(yan)上升管(guan)(guan)引至爐(lu)頂的輸(shu)氣總(zong)管(guan)(guan),通(tong)(tong)過(guo)輸(shu)氣總(zong)管(guan)(guan)將氣體送至二段(duan)(duan)(duan)轉(zhuan)化(hua)爐(lu),工(gong)藝流程(cheng)(cheng)如圖1所示。
發布時間: 2023-05-16 11:23
摘(zhai)要:河南金(jin)梅天(tian)慶煤化(hua)(hua)(hua)(hua)(hua)(hua)工(gong)有限(xian)責(ze)任公(gong)司“30·52·5”項目甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)裝(zhuang)置(zhi)采用(yong)(yong)英國戴維(wei)(Davy)公(gong)司的甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)工(gong)藝,主(zhu)甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)反應(ying)(ying)器內壁采用(yong)(yong)耐(nai)高(gao)(gao)溫澆(jiao)(jiao)注料(liao)砌筑(zhu)(zhu),試(shi)生產6個月時,主(zhu)甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)反應(ying)(ying)器塔壁出(chu)(chu)現嚴重超溫現象,系(xi)統被迫緊急停車處理(li),檢查發現主(zhu)甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)反應(ying)(ying)器耐(nai)高(gao)(gao)溫澆(jiao)(jiao)注料(liao)隔(ge)(ge)熱層存在澆(jiao)(jiao)筑(zhu)(zhu)質量缺(que)陷,需(xu)對(dui)其(qi)(qi)(qi)予以修復或重新(xin)(xin)(xin)澆(jiao)(jiao)筑(zhu)(zhu)。考慮修復效果可能(neng)不佳(jia)及(ji)重新(xin)(xin)(xin)澆(jiao)(jiao)筑(zhu)(zhu)施工(gong)周(zhou)期(qi)長(chang)、甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji)(并(bing)無鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua)縣里(li))可能(neng)報(bao)廢及(ji)其(qi)(qi)(qi)供貨(huo)周(zhou)期(qi)長(chang)(催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji)更換成(cheng)本高(gao)(gao)),晉(jin)煤天(tian)慶參考相關資料(liao)并(bing)結合系(xi)統生產實際,經(jing)分(fen)析與論證,決定(ding)將甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji)先鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua)、卸出(chu)(chu)、充氮(dan)氣密閉存放,待耐(nai)高(gao)(gao)溫澆(jiao)(jiao)注料(liao)隔(ge)(ge)熱層重新(xin)(xin)(xin)澆(jiao)(jiao)筑(zhu)(zhu)完畢(bi)后(hou)在回裝(zhuang)投用(yong)(yong),簡(jian)要介紹甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)裝(zhuang)置(zhi)流程及(ji)甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji)裝(zhuang)填情(qing)況(kuang),詳(xiang)細介紹甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji)的鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua)流程、鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua)步(bu)驟及(ji)其(qi)(qi)(qi)關鍵控制點。甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji)鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua)后(hou)再次回裝(zhuang)投用(yong)(yong)的情(qing)況(kuang)表明,其(qi)(qi)(qi)活性(xing)依然滿足工(gong)況(kuang)需(xu)要,鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua)處理(li)是(shi)成(cheng)功的,帶來的經(jing)濟效益是(shi)客觀的,可為業內類(lei)似(si)問題的處理(li)提供一些(xie)參考和借鑒。 關鍵詞:甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)裝(zhuang)置(zhi);主(zhu)甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)反應(ying)(ying)器;耐(nai)高(gao)(gao)溫澆(jiao)(jiao)筑(zhu)(zhu)料(liao)隔(ge)(ge)熱層缺(que)陷;重新(xin)(xin)(xin)澆(jiao)(jiao)筑(zhu)(zhu);甲(jia)(jia)(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)(hua)催(cui)(cui)化(hua)(hua)(hua)(hua)(hua)(hua)劑(ji)(ji);鈍(dun)(dun)(dun)化(hua)(hua)(hua)(hua)(hua)(hua);活性(xing)評價(jia)
發布時間: 2023-03-23 08:23
陳強,毛明明,高(gao)敏,李(li)佳 摘(zhai)要:近年(nian)來,氫(qing)氣(qi)在全球范(fan)圍內的需求量(liang)逐年(nian)上升,氫(qing)氣(qi)作為清潔能源受到人們(men)的重(zhong)(zhong)視。文章(zhang)對天然(ran)氣(qi)制(zhi)氫(qing)方法,天然(ran)氣(qi)制(zhi)氫(qing)鎳(nie)基催(cui)化(hua)劑(ji),以(yi)及熱回流(liu)(liu)(liu)技(ji)術(shu)做了綜(zong)述。甲(jia)烷蒸汽重(zhong)(zhong)整(zheng)技(ji)術(shu)已經成(cheng)熟,而甲(jia)烷部分氧化(hua)、干(gan)重(zhong)(zhong)整(zheng)、自熱重(zhong)(zhong)整(zheng)等制(zhi)氫(qing)技(ji)術(shu)仍處(chu)于發展階段,面臨著挑戰。由(you)于鎳(nie)活性高(gao),價格低廉是貴(gui)金屬的良好替代(dai)品,當前的制(zhi)氫(qing)催(cui)化(hua)劑(ji)仍以(yi)鎳(nie)基催(cui)化(hua)劑(ji)為主要選擇。熱回流(liu)(liu)(liu)技(ji)術(shu)主要介(jie)紹了單(dan)向流(liu)(liu)(liu)和逆流(liu)(liu)(liu)反應(ying)器對其熱回流(liu)(liu)(liu)的特(te)點,并對甲(jia)烷制(zhi)氫(qing)技(ji)術(shu)提出改(gai)進策略。 關(guan)鍵詞:天然(ran)氣(qi);制(zhi)氫(qing);催(cui)化(hua)劑(ji);回熱技(ji)術(shu)
發布時(shi)間: 2022-09-27 08:17
摘要:以采用Davy工(gong)藝(yi)(yi)的某180萬t/a大型(xing)煤制甲醇合成(cheng)裝(zhuang)(zhuang)置弛放氣經膜分離串聯變(bian)壓(ya)吸附(fu)制氫工(gong)段為例,介紹了變(bian)壓(ya)吸附(fu)制氫的裝(zhuang)(zhuang)置配置、工(gong)藝(yi)(yi)流程以及氫氣儲(chu)存、氫氣使用的操(cao)作流程、注意(yi)事(shi)項,闡述了變(bian)壓(ya)吸附(fu)制氫裝(zhuang)(zhuang)置的開車操(cao)作流程和(he)裝(zhuang)(zhuang)置在不同情況下停車的操(cao)作步驟,并(bing)指出其(qi)開停車及氫氣儲(chu)存、運(yun)輸等(deng)過程的注意(yi)事(shi)項。
發布時間: 2022-07-26 08:45
繆(mou)傳(chuan)耀 (匯智工(gong)程(cheng)科技股份有限公司武漢分(fen)公司,湖北(bei) 武漢 430000) 摘 要(yao):化(hua)工(gong)技術的(de)應(ying)用為(wei)社會(hui)經濟發展貢獻(xian)了很(hen)多(duo)化(hua)工(gong)制(zhi)品(pin),為(wei)人們(men)生(sheng)(sheng)產(chan)(chan)生(sheng)(sheng)活創造了很(hen)多(duo)便利(li)條件(jian),合(he)成氨在工(gong)業(ye)、農業(ye)及醫藥(yao)等諸多(duo)領域內均有應(ying)用。但因(yin)生(sheng)(sheng)產(chan)(chan)制(zhi)造技術的(de)制(zhi)約,造成當下的(de)合(he)成氨工(gong)藝(yi)實(shi)施過程(cheng)中存在著很(hen)大問題(ti)。從闡述煤(mei)氣(qi)化(hua)原理著手,總結煤(mei)化(hua)工(gong)合(he)成氨工(gong)藝(yi)的(de)基本流程(cheng),以實(shi)現節能生(sheng)(sheng)產(chan)(chan)為(wei)目標,探(tan)究幾點可行的(de)優(you)(you)化(hua)對策。 關鍵詞:煤(mei)化(hua)工(gong);合(he)成氨;工(gong)藝(yi)分(fen)析(xi);節能優(you)(you)化(hua)
發布時間: 2022-06-01 08:51
摘要:氧化(hua)(hua)(hua)(hua)鎂為(wei)載(zai)體的(de)(de)釕基氨(an)合成催(cui)(cui)化(hua)(hua)(hua)(hua)劑具有(you)潛在(zai)的(de)(de)工(gong)業(ye)應用(yong)前景,已(yi)引起了(le)人(ren)們(men)極大(da)的(de)(de)關(guan)注。制(zhi)備了(le)5種釕基催(cui)(cui)化(hua)(hua)(hua)(hua)劑Ru/MgO、Ru/γ-Al2O3、K-Ru/ MgO、Ba-Ru/MgO和(he)(he)K-Ba-Ru/MgO,在(zai)v(N2):v(H2) =1 :3,2.0MPa,24000h-1和(he)(he)653~873K反(fan)應條件下,評價了(le)它們(men)的(de)(de)合成氨(an)催(cui)(cui)化(hua)(hua)(hua)(hua)活(huo)性(xing),并(bing)對相關(guan)催(cui)(cui)化(hua)(hua)(hua)(hua)劑進行了(le)BET和(he)(he)XRD表征。結果表明:Ru/MgO的(de)(de)最高(gao)(gao)活(huo)性(xing)約(yue)為(wei)Ru/γ-Al2O3的(de)(de)2倍(bei),且最高(gao)(gao)活(huo)性(xing)反(fan)應溫(wen)度還(huan)低了(le)20 K;Ba組份的(de)(de)添(tian)加(jia)有(you)利于(yu)降低Ru/ MgO基催(cui)(cui)化(hua)(hua)(hua)(hua)劑的(de)(de)最高(gao)(gao)活(huo)性(xing)溫(wen)度;K-Ba-Ru/MgO在(zai)653K、Ba-Ru/MgO在(zai)773K、K-Ru/MgO和(he)(he)Ru/MgO在(zai)813K以上使用(yong)時,將更有(you)利于(yu)催(cui)(cui)化(hua)(hua)(hua)(hua)活(huo)性(xing)的(de)(de)發揮。因此,對于(yu)Ru/MgO基催(cui)(cui)化(hua)(hua)(hua)(hua)劑而(er)言,促進劑的(de)(de)添(tian)加(jia)應根據擬(ni)采用(yong)的(de)(de)操(cao)作溫(wen)度來決定。 關(guan)鍵詞:合成氨(an);Ru/MgO基催(cui)(cui)化(hua)(hua)(hua)(hua)劑;促進劑
發布(bu)時(shi)間: 2022-01-15 09:52
崔(cui)占磊 (中海(hai)油惠州(zhou)石(shi)化有限公(gong)司,廣東 惠州(zhou) 516086) 摘 要:制(zhi)(zhi)氫(qing)裝置停工過程是(shi)一項復雜(za)的系統工程,操(cao)作不當容易(yi)造成催(cui)(cui)化劑(ji)結碳、中毒(du)或(huo)粉碎,也容易(yi)造成設備損壞(huai)或(huo)使(shi)用(yong)壽命(ming)下(xia)降(jiang),甚至產生嚴重的安全環保(bao)事故,總結惠州(zhou)石(shi)化歷次停工經驗,從保(bao)護催(cui)(cui)化劑(ji)、保(bao)護設備、消除安全風(feng)(feng)險等方面(mian)出發,系統分析停工過程中的操(cao)作風(feng)(feng)險和注意(yi)(yi)事項,并針對性地(di)采取(qu)有效的控制(zhi)(zhi)措施,對于制(zhi)(zhi)氫(qing)裝置安全停工和長周(zhou)期穩(wen)定(ding)運行(xing)來(lai)說至關重要,對于所有烴類蒸汽轉化制(zhi)(zhi)氫(qing)裝置停工操(cao)作具有一定(ding)的借鑒和參考意(yi)(yi)義。 關鍵詞(ci):天然氣制(zhi)(zhi)氫(qing);操(cao)作風(feng)(feng)險;有效措施
發布時(shi)間: 2022-01-13 09:12
摘要(yao):采用浸漬(zi)法(fa)制備(bei)了(le)Ni/SSZ-13催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji),并(bing)研究了(le)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)的(de)CO2甲(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)反應性能。通過N2物(wu)理(li)吸(xi)附-脫附、X射線衍射、掃描電子顯(xian)微(wei)鏡、透射電子顯(xian)微(wei)鏡、X射線光電子能譜等表(biao)(biao)征分(fen)析方法(fa)對催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)的(de)額質(zhi)構特性及物(wu)理(li)化(hua)(hua)(hua)(hua)(hua)學性質(zhi)進(jin)行了(le)研究。結(jie)果表(biao)(biao)明,Ni/SSZ-13催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)在250℃開始(shi)表(biao)(biao)現出CO2甲(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)活(huo)性;在450℃,Ni-SSZ-14表(biao)(biao)現出最佳(jia)的(de)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)反應活(huo)性,CO2轉化(hua)(hua)(hua)(hua)(hua)率和(he)CH4選擇性分(fen)別為(wei)70%和(he)95%。SSZ-13載體表(biao)(biao)現出長方體結(jie)構,孔(kong)結(jie)構主(zhu)要(yao)為(wei)微(wei)孔(kong),并(bing)含有部分(fen)介(jie)孔(kong),為(wei)鎳物(wu)質(zhi)的(de)分(fen)散提供個較大的(de)比(bi)表(biao)(biao)面積。煅(duan)燒后(hou)的(de)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)在500℃的(de)還原過程中,NiO被還原成金屬(shu)Ni,金屬(shu)Ni是CO2甲(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua)的(de)主(zhu)要(yao)活(huo)性組分(fen)。 關鍵(jian)詞:二氧化(hua)(hua)(hua)(hua)(hua)碳;甲(jia)(jia)烷(wan)(wan)化(hua)(hua)(hua)(hua)(hua);Ni/SSZ-13催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji);反應性能
發布時(shi)間: 2022-01-01 09:37
任(ren)曉凈 (安徽華東化(hua)工(gong)醫藥工(gong)程有限責任(ren)公司上(shang)海分公司,上(shang)海 201315) 摘(zhai) 要(yao):主要(yao)對天然(ran)氣(qi)蒸汽轉(zhuan)化(hua)-變(bian)壓吸(xi)附(PSA)氫(qing)氣(qi)提(ti)純(chun)裝(zhuang)置(zhi)在(zai)生產不同氫(qing)氣(qi)純(chun)度、不同產氫(qing)規(gui)模(mo)的工(gong)況下進行能(neng)耗(hao)分析,從而為不同的需求客戶提(ti)供參考依據。 關(guan)鍵詞:天然(ran)氣(qi)蒸汽轉(zhuan)化(hua)-變(bian)壓吸(xi)附(PSA)氫(qing)氣(qi)提(ti)純(chun);不同氫(qing)氣(qi)純(chun)度;不同氫(qing)氣(qi)規(gui)模(mo);能(neng)耗(hao)分析
發布時間: 2021-12-28 09:17